NETZSCH Measurements
- Instrument
-
DSC 204 F1 Phoenix®
- Sample Mass
- 10.65 mg
- Isothermal Phase
- 8 min
- Heating/Colling Rates
- 10 K/min
- Crucible
- Al, piercec
- Atmosphere
- N2 (50 ml/min)
Evaluation
In the above graphics, only the 1st heating (blue) was evaluated since the effects in the 2nd heating − after controlled cooling – are no longer resolved.
In the 1st heating (blue curve), the glass transition occurs at -23°C (midpoint, with a change in specific heat of 0.56 J/(g·K)). It is followed by two overlapping, endothermal melting effects at 51°C and 87°C (peak temperatures). The entire heat of fusion of the combined peaks amounts to approx. 75 J/g.