NETZSCH Measurements
- Instrument
-
DSC 204 F1 Phoenix®
- Sample Mass
- 11.79 mg
- Isothermal Phase
- 5 min
- Heating/Colling Rates
- 10 K/min
- Crucible
- Al, pierced
- Atmosphere
- N2 (50 ml/min)
Evaluation
As an entirely amorphous thermoplastic, SAN has a glass transition in this case at 109°C (both heatings, midpoint each) with a step height (Δcp) of 0.40 J/(g.K) and 0.41 J/(g.K), respectively.
In the 2nd heating (green), the glass step shows a relaxation peak, indicating that short-range orders have formed in the polymer during the controlled cooling at 10 K/min. The thermomechanical history of the sample can be noticed in the DSC curve of the 1st heating (blue) by means of some slight waves.