NETZSCH Measurements
- Instrument
-
DSC 204 F1 Phoenix®
- Sample Mass
- 8.66 mg
- Isothermal Phase
- 8 min
- Heating/Colling Rates
- 10 K/min
- Crucible
- Al, pierced
- Atmosphere
- N2 (50 ml/min)
Evaluation
Shown in the 2nd heating (green) of this example is a broad, strongly structured endothermal melting transition with a distinctive pre-peak at 202°C and an additional shoulder at 173°C (peak temperatures). The temperature of the main effect (also peak temperature) occurred at 217°C. The total melting enthalpy was approx. 75 J/g.
The glass transition in the 2nd heating had a midpoint temperature of 40°C, at the lower end of the glass transition temperature for these materials. In the 1st heating (blue), the Tg midpoint was approximately 2 K lower and overlapped by a large
relaxation peak.