NETZSCH Measurements
- Instrument
-
DSC 204 F1 Phoenix®
- Sample Mass
- 12.06 mg
- Isothermal Phase
- 3 min/3 min/5 min
- Heating/Colling Rates
- 10 K/min
- Crucible
- Al, pierced
- Atmosphere
- N2 (50 ml/min)
Evaluation
A glass transition (here at 42°C, midpoint) and a clearly structured endothermal melting effect for the α (peak temperature 226°C) and β phase (peak temperature 217°C) in the 2nd heating (green) are characteristic of PBT. In the 1st heating (blue), the glass transition midpoint temperature of 44°C was comparable to that in the 2nd heating, but is overlapped with a relaxation peak. Prior to the melting transition, a post crystallization (small exothermal peak at 207°C) occurred in the 1st heating.