NETZSCH Measurements
- Instrument
-
DSC 204 F1 Phoenix®
- Sample Mass
- 11.12 mg
- Isothermal Phase
- 10 min
- Heating/Colling Rates
- 10 K/min
- Crucible
- Al, pierced
- Atmosphere
- N2 (40 ml/min)
Evaluation
The 1st heating (blue) shows a relaxation peak that obscures the glass transition and a melting peak with a shoulder (peak temperature 258°C). The glass transition with a midpoint temperature of 80°C is clearer in the 2nd heating (green). The shoulder is gone from the melting transition which peaks at 259°C.