NETZSCH Measurements
- Instrument
-
DSC 204 F1 Phoenix®
- Sample Mass
- 12.66 mg
- Isothermal Phase
- 5 min
- Heating/Colling Rates
- 10 K/min
- Crucible
- Al, pierced
- Atmosphere
- N2 (40 ml/min)
Evaluation
The glass transition of the amorphous PES occurred at 228°C (midpoint) with a step height of 0.23 J/(g.K) and 0.24 J/(g.K) in the 1st (blue) and 2nd heating (green), respectively. In the DSC curve of the 2nd heating, the glass transition step is overlapped by a small relaxation peak, indicating the presence of ordered regions within the amorphous matrix that formed during the controlled cooling at 10 K/min.