NETZSCH Measurements
- Instrument
-
DSC 204 F1 Phoenix®
- Sample Mass
- 26.26 mg
- Isothermal Phase
- 10 min
- Heating/Colling Rates
- 5 K/min/10 K/min cooling/20 K/min
- Crucible
- High-pressure steel crucibles, closed
- Atmosphere
- N2 (40 ml/min)
Evaluation
The 1st heating (blue ) shows a glass transition at approx. 48°C (midpoint) with an overlapping enthalpy relaxation, followed by a multi-step exothermal curing effect with peak temperatures of 141°C and 206°C and a total enthalpy of 191 J/g. In the
following 2nd heating (green), the glass transition shifted to approx. 72°C (midpoint) as a result of the extensive curing in the previous heating step.