NETZSCH Measurements
- Instrument
-
DSC 204 F1 Phoenix®
- Sample Mass
- 18.95 mg
- Isothermal Phase
- 5 min
- Heating/Colling Rates
- 10 K/min
- Crucible
- Al, pierced
- Atmosphere
- N2 (40 ml/min)
Evaluation
In the 1st heating, the glass transition at 107°C (midpoint) was followed by a broad, shallow, exothermal post-curing effect between approx. 120°C and 200°C (peak temperature 167°C). Due to the post-curing, the glass transition in the 2nd heating
(after controlled cooling) was approx. 4 K (midpoint temperature 111°C) higher.
The position of the glass transition temperature is directly related to the degree of curing.
The more extensive the post-curing, the more the glass transition shifts to higher temperatures.