NETZSCH Measurements
- Instrument
-
DSC 204 F1 Phoenix®
- Sample Mass
- 10.82 mg
- Isothermal Phase
- 5 min
- Heating/Colling Rates
- 10 K/min
- Crucible
- Al, pierced
- Atmosphere
- N2 (40 ml/min)
Evaluation
Due to the missing plasticizer the glass transition of the entirely amorphous plastic PVC-U occurred at much higher temperatures, compared to PVC-P; in the present case at approx. 84°C (in both heatings, midpoint) with a step height (Δcp) of 0.32 J/(g·K) in the 2nd heating. The slight waves, overlapping the glass transition step in the 1st heating, are probably due to stress in the material that is dissipated during thermal treatment.