NETZSCH Measurements
- Instrument
-
DSC 204 F1 Phoenix®
- Sample Mass
- 11.29 mg
- Isothermal Phase
- 3 min
- Heating/Colling Rates
- 10 K/min
- Crucible
- Al, pierced
- Atmosphere
- N2 (40 ml/min)
Evaluation
Polyamides can absorb humidity. This affects the position of the glass transition due to the plasticizing properties of water.
In the measuring curves shown above, a small peak can be seen in the 1st heating (blue) at 82°C, probably due to the evaporation of water. As a result, the glass transition temperature increases from 51°C in the 1st heating (blue, midpoint) to 53°C
in the 2nd heating (green, again midpoint).
Endothermal melting of the semi-crystalline polymer occurs at 184°C (peak temperature) in the 2nd heating with a melting enthalpy of 52 J/g.